尿素改性热塑性酚醛树脂的合成及应用

先用尿素、甲醛合成二羟甲脲，然后在酸性介质下把二羟甲脲滴加在苯酚中反应合成尿素改性的热塑性酚醛树脂。研究了反应浑浊点和二羟甲脲的滴加速度，同时研究了二羟甲脲与苯酚的尿酚比与物料的出料温度、产品产率及树脂理化性能指标的关系。结果表明：（1）二羟甲脲滴加速度的合适范围是0．012－0．029mol/mol.min；（2）本树脂的出料温度为125℃以下；（3）产品收率，游离酚，软化点随尿比的增长而递增，凝胶速度变化不大。另介绍了这种树脂在酚醛模塑料中的应用。     

Ways of strengthening biodegradable soy‐dreg plastics

Biodegradable plastics (GSD) based on soy dreg (SD) were prepared by compression‐molding, with glycerol as the plasticizer and glutaraldehyde (GA) as the cross‐linker. The structure and properties of the GSD sheets were investigated by Fourier‐transform infrared spectroscopy (FTIR), X‐ray diffraction (XRD), differential scanning calorimetry (DSC), dynamic mechanical thermal analysis (DMTA), scanning electron microscope (SEM), and tensile test methods. The results indicate that when GA content was 6.8%, the tensile strength (σ_b) of the sheet reached the maximum value of 14.5 MPa. Moreover, the strength and water resistance of the sheets coated with castor‐oil‐based polyurethane/nitrochitosan interpenetrating network (IPN) coating were significantly enhanced to 24.6 MPa in the dry state and 9.8 MPa in the wet state. Simultaneously, the test of biodegradability of the GSD sheet in a mineral salts medium containing microorganisms and agar proved that GSD could be fully biodegradable. This work has provided a novel way to utilize low‐cost SD to prepare biodegradable plastics. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 422–427, 2003     

An integrated approach to hypersonic entry attitude control

This paper presents an integrated approach based on dynamic inversion(DI)and active disturbance rejection control(ADRC)to the entry attitude control of a generic hypersonic vehicle(GHV).DI is frstly used to cancel the nonlinearities of the GHV entry model to construct a basic attitude controller.To enhance the control performance and system robustness to inevitable disturbances,ADRC techniques,including the arranged transient process(ATP),nonlinear feedback(NF),and most importantly the extended state observer(ESO),are integrated with the basic DI controller.As one primary task,the stability and estimation error of the second-order nonlinear ESO are analyzed from a brand new perspective:the nonlinear ESO is treated as a specifc form of forced Li′enard system.Abundant qualitative properties of the Li′enard system are utilized to yield comprehensive theorems on nonlinear ESO solution behaviors,such as the boundedness,convergence,and existence of periodic solutions.Phase portraits of ESO estimation error dynamics are given to validate our analysis.At last,three groups of simulations,including comparative simulations with modeling errors,Monte Carlo runs with parametric uncertainties,and a six degrees-of-freedom reference entry trajectory tracking are executed,which demonstrate the superiority of the proposed integrated controller over the basic DI controller.     

Novel Method To Optimize the Structure of Reticulated Porous Ceramics

A novel method has been developed for the fabrication of silicon nitride reticulated porous ceramics (RPCs) with regulated structure, using polyurethane sponge as the template. This technique includes two centrifuging steps. In the first stage, the polyurethane sponges are coated with thin slurry through high-speed centrifuging. After the slurry on sponges dried, a high-strength green body without filled cells is obtained. In the second stage, because of improved adhesion between the body and the slurry after the first coating, the body with uniformly thick strut is produced by recoating the as-prepared green body with thixotropic slurry and centrifuging again. The loading content of slurry and the pore diameter of the RPCs body greatly depend on the slurry viscosity in the process of recoating. The strut diameter and pore diameter of the RPCs are effectively optimized by modulating the slurry viscosity.     

古马隆树脂型聚氨酯防水涂料

介绍一种以古马隆树脂改性的新型双组分聚氨酯防水涂料，并对其原材料的选择、配方、生产工艺等方面进行了研究。     

面向内部威胁的最优安全策略算法研究

内部攻击行为具有很强的伪装性,这使得检测结果具有不确定性.攻击图模型经常用于描述攻击行为的多个攻击步骤之间的因果关系,但在计算最优安全策略时,很少考虑到当前观测事件所具有的不确定性,也没有从概率的角度刻画安全防护策略实施后对攻击成功概率带来的影响.在前人的概率攻击图模型研究基础上,首次提出了一种面向内部威胁的安全防护策略概率攻击图(measures probablitity attack graph,MPAG)模型,在该模型中较为完备地讨论了内部攻击的3类不确定性,并引入安全防护措施节点及其对攻击成功的概率影响.在该模型基础上,最优安全防护策略计算被证明是一个NP难问题,一种贪心算法被提出解决该问题,该算法能在多项式时间内动态计算近似最优安全防护策略集合.最后给出一个真实的内部威胁网络环境的概率攻击图实例,说明该模型及相应的贪心算法能根据当前观测事件及其置信概率,计算满足一定代价限制条件的近似最优安全防护策略集合.     

相容剂对聚丙烯／滑石粉增容作用研究

作者采用熔融接技方法制备PP-g-AA和PP-g-MAH,并比较了这两种相容剂对PP/滑石粉体系的增容效果。着重研究了引发剂含量、单体含量对PP-g-AA增容作用的影响以及PP-g-AA用量对PP/滑石粉体系力学强度的影响。     

共沉淀法制备纳米氧化镁的研究

以氯化镁与碳酸钠为原料,采用共沉淀法,研究了反应溶液的pH值、反应物浓度、反应温度、反应时间和煅烧温度对制备纳米氧化镁粉体的影响,通过透射电镜(TEM)、X射线衍射(XRD)、热重分析(TG)对样品的性能进行测试,获得纳米氧化镁平均粒径约12 nm,且分布较均匀.     

一种基于对等网络的云资源定位算法

提出用分布式哈希表(DHT)为每台云服务器产生一个唯一的节点编号,该编号作为网络拓扑结构、检索信息存储和信息查询共同的标志符,从而形成一个适合分布式计算的结构化P2P覆盖网.设计了新的拓扑和路由协议来解决云资源的常数跳定位问题.仿真实验表明,经典的P2P算法平均查找跳数与网络规模成正相关,无法依据云计算的实际需要人为地控制查找跳数;该算法的平均查找跳数与网络规模无关,随着网络规模的增大而趋向于设定值,可以解决云资源的常数跳定位问题.     

高职院校无线网络的规划与设计

高职院校一般规模比较小,WLAN就比较适合这个范围使用,通过无线网络可以很好的弥补目前有线网络的不足,使教职工和学生可以随时随地的进行网上办公和学习。通过需求分析,找到网络架设的重点;通过无线网络的安全性分析,使学校在购买相关设备的时候可以有所参考;通过无线网络的管理,使大家深刻认识到网络管理的重要性。